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I’ve seen articles about it on the web yet have read no actual write-ups or results of actual synthesis.
Yes - I did plenty of times.
The first step the acid catalyzed aldol condensation is easy and pretty good yields of the intermediate can be achieved.
Now the baeyer villiger Oxidation step is something I've been working on for a long time by now, trying all sorts of different catalysts and reagents. If you have access to something like commercial 40% peracetic acid solution (which I only can get once in a while and only in Limited amounts) then it's an easy and good route to P2P.
Also If you do have access to 30% hydrogen peroxide solutions its still a good route for smaller scale production.
If you're Just looking at producing small amounts of high quality P2P and Not worried about some effort then I guess its one of the best ways when you don't have access to restricted chemicals since everything you need can be bought otc or be produced in a proper Lab setting.
If you have any questions regarding any of the steps I am Sure i can Help. Also got plenty of footage/Pics to illustrate the process.
Yes - I did plenty of times.
The first step the acid catalyzed aldol condensation is easy and pretty good yields of the intermediate can be achieved.
Now the baeyer villiger Oxidation step is something I've been working on for a long time by now, trying all sorts of different catalysts and reagents. If you have access to something like commercial 40% peracetic acid solution (which I only can get once in a while and only in Limited amounts) then it's an easy and good route to P2P.
Also If you do have access to 30% hydrogen peroxide solutions its still a good route for smaller scale production.
If you're Just looking at producing small amounts of high quality P2P and Not worried about some effort then I guess its one of the best ways when you don't have access to restricted chemicals since everything you need can be bought otc or be produced in a proper Lab setting.
If you have any questions regarding any of the steps I am Sure i can Help. Also got plenty of footage/Pics to illustrate the process.
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